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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2112105Generated: November 3, 2026

Hydrochloric Acid → HCID 55234162, compound

https://huagongshe.com/reaction/2112105

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 63670490HCID 63670490—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 55234162HCID 55234162—

Reaction Steps

200 mg (0.716 mmol) (3-methoxy-4-nitro-phenyl)-(3-pyrrolidin-1-yl-propyl)-amine are dissolved in 10 ml of methanol and combined with 537 μl (2.148 mmol) dioxanic hydrochloric acid and 20 mg palladium on charcoal. The reaction mixture is stirred for 1 h at ambient temperature and 5 bar H2 pressure. The catalyst is filtered off and the solvent is eliminated in vacuo.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07521457B2
Source datasetuspto-grants-2009_04
ORD IDord-d8358bcd273d4e8d94122873bff73054
Source noteuspto-grants-2009_04