HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86608936, compound → HCID 86608935, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86608936 | HCID 86608936 | — |
| Solvent | Acetyl chloride | HCID 6367 | — |
| Product | HCID 86608935 | HCID 86608935 | — |
Reaction Steps
To a mixture of the product from Example 14 (100 mg, 0.28 mmol) in acetyl chloride/glacial acetic acid (3 mL, 1:2, v/v) is stirred at room temperature until disappearance of the starting nucleoside, as judged by TLC. The mixture is evaporated in vacuo to dryness and purified on silica gel column.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524825B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-ca3568e4e2ed4700afc4111cc807dfbf |
| Source note | uspto-grants-2009_04 |