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HRID2112444

反应详情

EQUATION

反应方程式

HRID 2112444 的结构方程式

REACTANTS

反应物

2
结构：O=S(=O)(Cl)c1cccc2ccccc12
HCID66560

1-Naphthalenesulfonyl chloride

C10H7ClO2S

结构：CC(C)(C)OC(=O)N1CCN(c2cccc3[nH]ccc23)CC1
HCID22015386

tert-Butyl 4-(1H-indol-4-yl)piperazine-1-carboxylate

C17H23N3O2

PRODUCTS

生成物

1
结构：Cl.O=S(=O)(c1cccc2ccccc12)n1ccc2c(N3CCNCC3)cccc21
HCID10113364

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according 4-(4-boc-piperazinyl)-indole and naphthylsulfonylchloride according to Method 3: 1H NMR (270 MHz DMSO-d6) δ 9.03 (br, 1H), 8.63 (d, J=8 Hz, 1H), 8.43 (d, J=8 Hz, 1H, 8.34 (d, J=8 Hz, 1H), 8.15-8.05 (m, 2H), 7.80-7.65 (m, 3H), 7.41 (d, J=8 Hz, 1H) 7.18 (t, J=8 Hz, 1H), 6.93 (d, J=5 Hz, 1H), 6.74 (d, J=8 Hz, 1H), 3.30-3.20 (m, 8H); MS (ESI+) for m/z 392 (M+H)+.