2-Methoxybenzaldehyde → HCID 57642319, compound

HRID 2112474Notes

Reaction equation

[CH3:1][O:2][C:3]1[CH:10]=[CH:9][CH:8]=[CH:7][C:4]=1[CH:5]=[O:6].[CH3:11][O:12][C:13]1[CH:14]=[C:15]([CH:17]=[CH:18][C:19]=1[O:20][CH3:21])[NH2:16]>>[NH2:16][C:15]1[CH:14]=[C:13]([O:12][CH3:11])[C:19]([O:20][CH3:21])=[CH:18][C:17]=1[C:5]([C:4]1[CH:7]=[CH:8][CH:9]=[CH:10][C:3]=1[O:2][CH3:1])=[O:6]

Participants

Reactant 2

HCID 86582-Methoxybenzaldehyde

HCID 227703,4-Dimethoxyaniline

Product 1

HCID 57642319HCID 57642319, compound

Procedure

(2-amino-4,5-dimethoxyphenyl)-(2-methoxyphenyl)-methanone (Xaa) was prepared by reacting 2-methoxybenzaldehyde with 0.0196 moles of 3,4-dimethoxy aniline in a manner analogous to Example 1. MH+/Z=288.

Sources & evidence

ORD record: ord-88adf7a2c63e4acf96ac5e24704c82e9
Source dataset: uspto-grants-2009_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07524840B2

Reaction notes

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