HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lawesson's reagent → HCID 57642352, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 57642377 | HCID 57642377 | — |
| Product | HCID 57642352 | HCID 57642352 | — |
Reaction Steps
5-(2-chlorophenyl)-7-cyano-1,3-dihydro-8-(2-(2-methoxyethoxy)ethoxy)-2H-1,4-benzodiazepin-2-thione (IIn) was prepared by reacting 0.00089 moles of 5-(2-chlorophenyl)-7-cyano-1,3-dihydro-8-(2-(2-methoxyethoxy)ethoxy)-2H-1,4-benzodiazepin-2-one (lactam In) with Lawesson's reagent in a manner analogous to Example 38. MH+/Z=430.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524840B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-f4d414a75ff94248b1cd4711d9a0ba81 |
| Source note | uspto-grants-2009_04 |