huagongshe.com
HRID2112511

反应详情

EQUATION

反应方程式

HRID 2112511 的结构方程式

REACTANTS

反应物

3
结构：NN
HCID9321

Hydrazine

H4N2

结构：COC(C)(OC)N(C)C
HCID87835

1,1-Dimethoxyethyl(dimethyl)amine

C6H15NO2

结构：COc1cc2c(cc1F)C(c1ccccc1Cl)=NCC(=S)N2
HCID57642343

未命名化合物

PRODUCTS

生成物

1
结构：COc1cc2c(cc1F)C(c1ccccc1Cl)=NC1=C(C)NNC1=N2
HCID178486441

未命名化合物

PROCEDURE

实验过程

5-(2-chlorophenyl)-1,2-dihydro-7-fluoro-8-methoxy-3-methyl-pyrazolo[3,4-b][1,4]benzodiazepine (IVa) was prepared by reacting 0.0224 moles of 5-(2-chlorophenyl)-1,3-dihydro-7-fluoro-8-methoxy-2H-1,4-benzodiazepin-2-thione (IIa) with 1,1-dimethoxy-N,N-dimethyl-ethanamine and then hydrazine in a manner analogous to Example 55. MH+/Z=357.