HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 178421676, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Reactant | HCID 57642389 | HCID 57642389 | — |
| Product | HCID 178421676 | HCID 178421676 | — |
Reaction Steps
5-(2-chlorophenyl)-1,2-dihydro-7-fluoro-8-(1-methylethoxy)-3-methyl-pyrazolo[3,4-b][1,4]benzodiazepine (IVh) was prepared by reacting 0.00198 moles of 5-(2-chlorophenyl)-1,3-dihydro-7-fluoro-8-(1-methylethoxy)-2H-1,4-benzodiazepin-2-thione (IIh) with 1,1-dimethoxy-N,N-dimethyl-ethanamine and then hydrazine in a manner analogous to Example 55. MH+/Z=385.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524840B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-65ebdac3c57e4d0daa3f40843970e34e |
| Source note | uspto-grants-2009_04 |