HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl 4-[2-(3-ethynylphenyl)-2-(1-hydroxycyclohexyl)ethyl]piperazine-1-carboxylate → HCID 86599398, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl 4-[2-(3-ethynylphenyl)-2-(1-hydroxycyclohexyl)ethyl]piperazine-1-carboxylate | HCID 86599048 | — |
| Reactant | HCID 86599399 | HCID 86599399 | — |
| Product | HCID 86599398 | HCID 86599398 | — |
Reaction Steps
In an analogous manner to Example 135, step 4, 1-[1-(3-ethynylphenyl-2-piperazin-1-ylethyl]cyclohexanol dihydrochloride was prepared from tert-butyl 4-[2-(3-ethynylphenyl)-2-(1-hydroxycyclohexyl)ethyl]piperazine-1-carboxylate. MS (ESI) m/z 313 ([M+H]+); HRMS: calcd for C20H28N2O+H, 313.2280; found (ESI, [M+H]+), 313.2280.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524846B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-f4fe6f82a31147f6a80ecf38fabe2bfc |
| Source note | uspto-grants-2009_04 |