HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 86605134, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86605133 | HCID 86605133 | — |
| Product | HCID 86605134 | HCID 86605134 | — |
Reaction Steps
[1-[7-(2-Butynyl)-2-chloro-9-methyl-8-oxo-8,9-dihydro-7H-purin-6-yl]piperazin-3-yl]c arbamic acid t-butyl ester (15 mg) was dissolved in trifluoroacetic acid. This reaction solution was stirred at room temperature for five minutes, and then concentrated. The residue was purified by reverse phase high performance liquid chromatography to give the title compound (7.23 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524847B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-cac4d2c0d42a4369b5d0cc37546972c5 |
| Source note | uspto-grants-2009_04 |