HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 68823841, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 57642817 | HCID 57642817 | — |
| Product | HCID 68823841 | HCID 68823841 | — |
Reaction Steps
4-[7-(2-Butynyl)-9-(1-methyl-6-oxo-1,6-dihydro-pyridin-3-yl)-8-oxo-8,9-dihydro-7H-purin-6-yl]piperazine-1-carboxylic acid t-butyl ester (15 mg) was dissolved in trifluoroacetic acid, and this reaction solution was stirred at room temperature for five minutes and then concentrated. The residue was purified by reverse phase high performance liquid chromatography to give the title compound (10.52 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524847B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-1fea6fedbace4346b2039998d1322f73 |
| Source note | uspto-grants-2009_04 |