HuagongsheHuagongshe Chemistry Print Report · For research reference only
Veratrylamine → HCID 68839477, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Veratrylamine | HCID 79832 | — |
| Reactant | 7-Bromo-2-(3-ethyl-ureido)-[1,2,4]triazolo[1,5-a]pyridine-5-carboxylic acid ethyl ester | HCID 57643068 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68839477 | HCID 68839477 | — |
Reaction Steps
7-Bromo-2-(3-ethyl-ureido)-[1,2,4]triazolo[1,5-a]pyridine-5-carboxylic acid ethyl ester, which may be prepared as in Example 6, (253 mg, 0.714 mmol) and 3,4-dimethoxybenzylamine (0.55 mL) were taken up in ethanol (4.0 mL). After 24 h the precipitate was removed by filtration and washed with ethanol to afford 7-bromo-2-(3-ethyl-ureido)-[1,2,4]triazolo[1,5-a]pyridine-5-carboxylic acid 3,4-dimethoxy-benzylamide MS (APCI+): m/z 478.4 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524860B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-4c102188abff4dca8b9bfebb2a793c35 |
| Source note | uspto-grants-2009_04 |