Methanol → HCID 68836863, compound

Participants

Reaction Steps

A suspension of the product of Step 1 (376 mg, 1.16 mmol) in DMF (4 mL) was treated with TosNCO (0.25 g, 1.3 mmol), then microwaved at 60° C. for 5 min. After stirring at room temperature for 18 h, MeOH (5 mL) was added and the resulting precipitate was collected by filtration and dried in vacuo to yield 1-tosyl-3-[5-(1-methyl-piperidin-4-ylamino)-7-pyridin-3-yl-[1,2,4]triazolo[1,5-a]pyridin-2-yl]-urea.

Provenance & Evidence