HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Butanesulfonyl chloride → HCID 69037715, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Butanesulfonyl chloride | HCID 75430 | — |
| Reactant | 3-Amino-6-methyl-1-(tert-butoxycarbonylmethyl)-2-pyridinone | HCID 10490115 | — |
| Product | HCID 69037715 | HCID 69037715 | — |
Reaction Steps
The title compound was prepared from tert-butyl 2-[3-amino-6-methyl-2-oxo-1(2H)-pyridinyl]acetate (EXAMPLE 1, STEP 1-3), and 1-butanesulfonyl chloride using the procedure of EXAMPLE 9 (STEP 2). The product was recrystallized from ethylacetate to give a white crystalline solid compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524871B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-847a9db6abed4dd0aa234b477f940c29 |
| Source note | uspto-grants-2009_04 |