HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloroaniline → HCID 10386765, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloroaniline | HCID 7812 | — |
| Reactant | HCID 59671878 | HCID 59671878 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 10386765 | HCID 10386765 | 97% |
Reaction Steps
10 g of the compound obtained in step A) are dissolved in 45 ml of anhydrous ethanol in the presence of 4.1 g of 4-chloroaniline. The mixture is heated at the reflux point of the ethanol for 3 days. After evaporating off the solvent, the expected product is crystallized from an isopropanol/ethanol mixture. 12.5 g of white crystals are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07524971B2 |
| Source dataset | uspto-grants-2009_04 |
| ORD ID | ord-1fc74aacb7d44d94b4d1e27a7139e3b4 |
| Source note | uspto-grants-2009_04 |