HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 68406876, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluoro-5-methylbenzonitrile | HCID 2774584 | — |
| Reactant | HCID 178418800 | HCID 178418800 | — |
| Product | HCID 68406876 | HCID 68406876 | — |
Reaction Steps
In analogy to example 5a, 2-fluoro-5-methyl-benzonitrile was reacted with 4-methylimidazole and potassium carbonate for 16 h at 90° C. After aqueous workup the title compound was obtained as a white solid (yield: 48%). MS: m/e=198.4 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432256B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-048c501b647b414bb21489163d0f40be |
| Source note | uspto-grants-2008_10 |