HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 67549463, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2-Fluorobenzonitrile | HCID 67855 | — |
| Reactant | HCID 178418800 | HCID 178418800 | — |
| Product | HCID 67549463 | HCID 67549463 | — |
Reaction Steps
In analogy to example 5a, 2-fluoro-benzonitrile was reacted with 4-methylimidazole and potassium carbonate for 16 h at 90° C. After aqueous workup the title compound was obtained as a white solid (yield: 60%). MS: m/e=184.2 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07432256B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-80051b26a20b48e7bcbf76197f61646f |
| Source note | uspto-grants-2008_10 |