HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 58786867, compound → HCID 21098182, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 58786867 | HCID 58786867 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Solvent | Palladium | HCID 23938 | — |
| Product | HCID 21098182 | HCID 21098182 | — |
Reaction Steps
1-Benzyl 4-tert-butyl 2-[5-(benzoyloxy)-4-(methoxycarbonyl)-1-methyl-6-oxo-1,6-dihydropyrimidin-2-yl]-2-methylpiperazine-1,4-dicarboxylate was dissolved in AcOEt (20 ml/mmol) and hydrogenated at atm pressure on 10% (w/w) Pd/C over night. After filtration of the catalyst, solvent was evaporated to give crude product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435734B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-98190c1ec88e4180be407c3998f2b7e7 |
| Source note | uspto-grants-2008_10 |