HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(Trifluoromethyl)benzoyl chloride → HCID 22147893, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(Trifluoromethyl)benzoyl chloride | HCID 67607 | — |
| Reactant | HCID 22147869 | HCID 22147869 | — |
| Reactant | 2-(3-Chloro-thiophen-2-yl)-2-oxo-1-ethylamine hydrochloride | HCID 69249884 | — |
| Product | HCID 22147893 | HCID 22147893 | — |
Reaction Steps
N-(2-(3-Chloro-thiophen-2-yl)-2-oxo-ethyl]4-trifluoromethyl-benzamide: The title compound was prepared from 2-(3-chloro-thiophen-2-yl)-2-oxo-1-ethylamine hydrochloride and 4-trifluoromethyl-benzoyl chloride by a procedure similar to Example 98a as a white solid (0.044 g, 30%). 1H NMR (DMSO-d6): 9.06 (m, 1H), 7.99 (m, 3H), 7.77 (d, J=8.4 Hz, 2H), 7.20 (d, J=9.0 Hz, 1H), 4.73 (s, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435750B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-81836bc646724b75a22c6c21cd45c864 |
| Source note | uspto-grants-2008_10 |