HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 2-[4-(4-Chloro-phenoxy)-piperidin-1-yl]-2-oxo-N-(2-oxo-2,3-dihydro-benzothiazol-6-yl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 4-(4-Chlorobenzyl)piperidine | HCID 3732780 | — |
| Reactant | N-(2-oxo-2,3-dihydro-benzothiazol-6-yl)-oxalamic acid | HCID 53306726 | — |
| Product | 2-[4-(4-Chloro-phenoxy)-piperidin-1-yl]-2-oxo-N-(2-oxo-2,3-dihydro-benzothiazol-6-yl)-acetamide | HCID 10137641 | — |
Reaction Steps
The title compound is prepared from N-(2-oxo-2,3-dihydro-benzothiazol-6-yl)-oxalamic acid (Example 61b) and 4-(4-chloro-benzyl)-piperidine according to the method described in Example 1c. Melting Point: 245-247° C. (diethylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-33c6d3f6510246638d6eb0a8d01b748f |
| Source note | uspto-grants-2008_10 |