HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(4-Methylphenoxy)piperidine → N-(2-Mercapto-3H-benzimidazol-5-yl)-2-(4-p-tolyloxy-piperidin-1-yl)-2-oxo-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(4-Methylphenoxy)piperidine | HCID 3837497 | — |
| Reactant | Oxo[(2-sulfanylidene-2,3-dihydro-1H-benzimidazol-5-yl)amino]acetic acid | HCID 178526016 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-(2-Mercapto-3H-benzimidazol-5-yl)-2-(4-p-tolyloxy-piperidin-1-yl)-2-oxo-acetamide | HCID 178426789 | — |
Reaction Steps
The title compound is prepared from N-(2-mercapto-3H-benzimidazol-5-yl)-oxalamic acid (Example 60b) and 4-p-tolyloxy-piperidine according to the method described in Example 1c. Melting Point: 311-314° C. (diethylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-044f03961fbb4026a04fa3caef4d30ce |
| Source note | uspto-grants-2008_10 |