HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → 2-[4-[3-Methyl-benzyl)-piperidin-1-yl]-2-oxo-N-(2-oxo-2,3-dihydro-benzoxazol-6-yl)-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | 4-(3-Methyl-benzyl)-piperidine | HCID 11159793 | — |
| Reactant | N-(2-oxo-2,3-dihydro-benzoxazol-6-yl)-oxalamic acid | HCID 53306576 | — |
| Product | 2-[4-[3-Methyl-benzyl)-piperidin-1-yl]-2-oxo-N-(2-oxo-2,3-dihydro-benzoxazol-6-yl)-acetamide | HCID 10200584 | — |
Reaction Steps
The title compound is prepared from N-(2-oxo-2,3-dihydro-benzoxazol-6-yl)-oxalamic acid (Example 43e) and 4-(3-methyl-benzyl)-piperidine according to the method described in Example 2. Melting Point: 204-208° C. (diisopropylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-a87dcc3ab28f429989ba451c543f0663 |
| Source note | uspto-grants-2008_10 |