4-(2-Phenylethyl)piperidine → 2-(4-Phenethyl-piperidin-1-yl)-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-7-yl)-acetamide

Participants

Role	Name	HCID	Charge
Reactant	4-(2-Phenylethyl)piperidine	HCID 4341895	—
Reactant	2-chloro-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl)-acetamide	HCID 24298282	—
Solvent	Diethyl Ether	HCID 3283	—
Product	2-(4-Phenethyl-piperidin-1-yl)-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-7-yl)-acetamide	HCID 69100649	—

Reaction Steps

The title compound is prepared from 2-chloro-N-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazine-7-yl)-acetamide (Example 153a) and 4-phenethyl-piperidine according to the method described in Example 142b. Melting Point: 200-203° C. (diethylether)

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US07435744B2
Source dataset	uspto-grants-2008_10
ORD ID	ord-6bb7b93428fd46cba9d9846b3c8177dd
Source note	uspto-grants-2008_10