HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → HCID 69100720, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | HCID 69100145 | HCID 69100145 | — |
| Solvent | Diethylether ethylacetate | HCID 21584169 | — |
| Product | HCID 69100720 | HCID 69100720 | — |
Reaction Steps
The title compound is prepared from N-(3-amino-phenyl)-2-[4-(4-fluoro-benzyl)-piperidin-1-yl]-acetamide dihydrochloride (Example 183) and methanesulfonyl chloride according to the method described in Example 176. Melting Point: 85-90° C. (dec.) (diethylether- ethyl acetate)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-d7ecd144e5454f7e9c6acb566533a607 |
| Source note | uspto-grants-2008_10 |