HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Ether → 2-(4-p-Tolyloxy-piperidin-1-yl)-2-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl-amino)-ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 7-amino-3,4-dihydro-2H-1,4-benzoxazin-3-one | HCID 2764182 | — |
| Reactant | 2-Chloro-1-(4-p-tolyloxy-piperidin-1-yl) ethanone | HCID 69100302 | — |
| Product | 2-(4-p-Tolyloxy-piperidin-1-yl)-2-(3-oxo-3,4-dihydro-2H-benzo[1,4]oxazin-7-yl-amino)-ethanone | HCID 86593934 | — |
Reaction Steps
The title compound is prepared from 7-amino-4H-benzo[1,4]oxazin-3-one and 2-chloro-1-(4-p-tolyloxy-piperidin-1-yl) ethanone (Example 208a) according to the method described in Example 206. Melting Point: 223-224° C. (diethylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-d1e2f6f4283f47d4bbd295a663b9aa74 |
| Source note | uspto-grants-2008_10 |