HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Anisidine → 1-[4-(4-Chloro-phenoxy)-piperidin-1-yl]-2-(4-methoxy-phenylamino)-ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Anisidine | HCID 7732 | — |
| Reactant | 6-{2-[4-(4-Chloro-phenoxy)-piperidin-1-yl]-2-oxo-ethylamino}-3h-benzoxazol-2-one | HCID 69099990 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-[4-(4-Chloro-phenoxy)-piperidin-1-yl]-2-(4-methoxy-phenylamino)-ethanone | HCID 69100564 | — |
Reaction Steps
The title compound is prepared from 2-chloro-1-[4-(4-chloro-phenoxy)-piperidin-1-yl]-ethanone (Example 233) and 4-methoxy-aniline according to the method described in Example 206. Melting Point: 127-130° C. (diethylether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435744B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1e8cf7ab1ca34ce5878ba2e16650b419 |
| Source note | uspto-grants-2008_10 |