HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 46218137, compound → HCID 72569092, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 46218137 | HCID 46218137 | — |
| Reactant | HCID 68639007 | HCID 68639007 | — |
| Reactant | HCID 86593153 | HCID 86593153 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 72569092 | HCID 72569092 | 82.2% |
Reaction Steps
200 mg (0.40 mmol) of product 9 and 340 mg (0.79 mmol) of Fmoc -p-azido-Phe-OH 10 (Bachem) are solved in 4 ml DMF (dimethylformamide) and reacted according to production of product 8. 300 mg (82%) of product 11 is obtained in form of an amorphic solid compound: C54H53N7O7 (912.07) MS (ESI+) 912.5 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435727B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1ba2fa475b0c49ccb765ffa77e34b380 |
| Source note | uspto-grants-2008_10 |