2-Chlorobenzaldehyde → HCID 11281991, compound

Participants

Reaction Steps

Following the protocol for Example 15, and substituting 3-[(4-methoxy-phenyl)-thiophen-3-yl-methylene]-8-aza-bicyclo[3.2.1]octane for 3-[(3-methoxy-phenyl)-thiophen-3-yl-methylene]-8-aza-bicyclo[3.2.1]octane and 2-chlorobenzaldehyde for 2-methylbenzaldehyde the title compound was obtained; MS m/z (MH+) 437; 1H NMR 300 MHz (MeOD-d4) δ 6.80-7.67 (m, 11H), 3.76 (s, 3H), 3.71 (s, 2H), 3.21-3.30 (m, 2H), 2.01-2.48 (m, 6H), 1.61-1.68 (m, 2H).

Provenance & Evidence