2-Thiophenecarboxaldehyde → HCID 11188998, compound

Participants

Reaction Steps

Following the protocol for Example 15, and substituting 3-[(4-methoxy-phenyl)-thiophen-3-yl-methylene]-8-aza-bicyclo[3.2.1]octane for 3-[(3-methoxy-phenyl)-thiophen-3-yl-methylene]-8-aza-bicyclo[3.2.1]octane and thiophene-2-carboxaldehyde for 2-methylbenzaldehyde the title compound was obtained; MS m/z (MH+) 408; 1H NMR 300 MHz (CDCl3) δ 6.81-7.29 (m, 10H), 3.79 (s, 2H), 3.78 (s, 3H), 3.24-3.33 (m, 2H), 2.22-2.54 (m, 4H), 1.91-2.04 (m, 2H), 1.58- 1.64 (m, 2H).

Provenance & Evidence