p-Toluidine → HCID 10454167, compound
Reaction equation
Br[CH2:2][C:3]([N:5]([CH2:8][CH3:9])[CH2:6][CH3:7])=[O:4].[NH2:10][C:11]1[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=1.[Cl:18][C:19]1[CH:20]=[C:21]([S:26](Cl)(=[O:28])=[O:27])[CH:22]=[CH:23][C:24]=1[CH3:25]>>[Cl:18][C:19]1[CH:20]=[C:21]([S:26]([N:10]([C:11]2[CH:16]=[CH:15][C:14]([CH3:17])=[CH:13][CH:12]=2)[CH2:2][C:3]([N:5]([CH2:8][CH3:9])[CH2:6][CH3:7])=[O:4])(=[O:28])=[O:27])[CH:22]=[CH:23][C:24]=1[CH3:25]Participants
4
Procedure
prepared by reaction of 2-bromo-N,N-diethylacetamide with p-toluidine and 3-chloro-4-methyl-benzenesulfonyl chloride
Sources & evidence
- ORD record
- ord-89a3ffd3183643409c5939289c3825c9
- Source dataset
- uspto-grants-2008_10
- Patent number
- US07435815B2
Reaction notes
Loading…