HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
p-Toluidine → 5-Isopropyl-pyridine-2-sulfonic acid p-tolylamide
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | p-Toluidine | HCID 7813 | — |
| Edukt | 2-bromo-N,N-diethylacetamide | HCID 225545 | — |
| Edukt | 5-Isopropylpyridine-2-sulfonyl chloride | HCID 22281918 | — |
| Produkt | 5-Isopropyl-pyridine-2-sulfonic acid p-tolylamide | HCID 58978419 | — |
Reaktionsschritte
prepared by reaction of 2-bromo-N,N-diethylacetamide with p-toluidine and 5-isopropyl-pyridine-2-sulfonyl chloride; in contrast to the general procedure the intermediate 5-isopropyl-pyridine-2-sulfonic acid p-tolylamide was isolated and crystallized from methanol/water 10/1
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07435815B2 |
| Quelldatensatz | uspto-grants-2008_10 |
| ORD ID | ord-734e169ad8884674a7914955fd8abf22 |
| Quellennotiz | uspto-grants-2008_10 |