HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 58978445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | N-(4-Methylphenyl)-N-[(1,2,3,4-tetrahydro-7-isoquinolinyl)sulfonyl]glycine | HCID 66885820 | — |
| Reactant | HCID 86615720 | HCID 86615720 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 58978445 | HCID 58978445 | — |
Reaction Steps
prepared by reaction of [(1,2,3,4-tetrahydro-isoquinoline-7-sulfonyl)-p-tolyl-amino]-acetic acid with diethylamine; due to the presence of formic acid in the eluent of the HPLC chromatography the product contained considerable amounts of N,N-diethyl-2-[(2-formyl-1,2,3,4-tetrahydro-isoquinoline-7-sulfonyl)-p-tolyl-amino]-acetamide (LC-MS: rt=0.91 min, 444 (M+1, ES+))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435815B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-3083c4eb2ace494ca2579974fd4cc55f |
| Source note | uspto-grants-2008_10 |