HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-(pyridin-2-ylmethyl)ethanamine → HCID 11754828, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-(pyridin-2-ylmethyl)ethanamine | HCID 4723804 | — |
| Reactant | N-(4-Methylphenyl)-N-[(1,2,3,4-tetrahydro-7-isoquinolinyl)sulfonyl]glycine | HCID 66885820 | — |
| Reactant | HCID 86615721 | HCID 86615721 | — |
| Solvent | Formic Acid | HCID 284 | — |
| Product | HCID 11754828 | HCID 11754828 | — |
Reaction Steps
prepared by reaction of [(1,2,3,4-tetrahydro-isoquinoline-7-sulfonyl)-p-tolyl-amino]-acetic acid with ethyl-pyridin-2-ylmethyl-amine; due to the presence of formic acid in the eluent of the HPLC chromatography the product contained considerable amounts of N-ethyl-2-[(2-formyl-1,2,3,4-tetrahydro-isoquinoline-7-sulfonyl)-p-tolyl-amino]-N-pyridin-2-ylmethyl-acetamide (LC-MS: rt=0.77 min, 507 (M+1, ES+))
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435815B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-c0133d9ba79643baa6342751f7e70d76 |
| Source note | uspto-grants-2008_10 |