反应详情

Dodecanethiol (246 g) and sodium methylate in methanol 30% (216 g) are charged to a rotary evaporator. Vacuum is applied and the solvent is abstracted completely using a bath temperature up to 90° C. The remaining sodium dodecanethiolate (272 g) is used without further purification in the subsequent step.

1. customup to 90° C
2. customThe remaining sodium dodecanethiolate (272 g) is used without further purification in the subsequent step