HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Dodecanethiol → Sodium dodecane-1-thiolate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Dodecanethiol | HCID 8195 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Sodium dodecane-1-thiolate | HCID 23672953 | — |
Reaction Steps
Dodecanethiol (246 g) and sodium methylate in methanol 30% (216 g) are charged to a rotary evaporator. Vacuum is applied and the solvent is abstracted completely using a bath temperature up to 90° C. The remaining sodium dodecanethiolate (272 g) is used without further purification in the subsequent step.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435854B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-e065efd27bdc4ae29861cdebd52379cf |
| Source note | uspto-grants-2008_10 |