HRID2115796

反应详情

EQUATION

反应方程式

HRID 2115796 的结构方程式

PROCEDURE

实验过程

6-(2-Fluoropyrimidin-4-yloxy)-1-naphthoic acid (1.2 g, 4.2 mmol) was dissolved in NH4OH (37% water, 20 mL) and stirred at RT for 3 h. Solvent was evaporated. A little bit of MeOH was added to the slurry followed by ether until the compound crashed out. Solid was filtered.

WORKUP

后处理

  1. customSolvent was evaporated
  2. additionA little bit of MeOH was added to the slurry
  3. filtrationSolid was filtered