Trimethylsilyl iodide → HCID 11413493, compound

Participants

Reaction Steps

The title compound was prepared (0.172 g, 78%) following the general procedure of Example 129 as a light yellow solid, hydrochloride salt from (+)-benzyl {[7-pyridin-3-yl-2,3-dihydro-1-benzofuran-2-yl]methyl}carbamate (0.33 g, 0.91 mmol) and trimethylsilyl iodide (0.73 g, 3.64 mmol). [α]D25=−20.4 (c 10.0 in methanol); mp 168-171° C.

Provenance & Evidence