HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 69107769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86599144 | HCID 86599144 | — |
| Product | HCID 69107769 | HCID 69107769 | — |
Reaction Steps
The title compound was prepared (0.137 g, 68%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[7-(2,4-difluorophenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.366 g, 0.88 mmol) and methylamine (0.273 g, 8.80 mmol). mp 156-160° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-26a62cb98baa4f6a908ad4cf5bd25725 |
| Source note | uspto-grants-2008_10 |