HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 15941774, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86599103 | HCID 86599103 | — |
| Product | HCID 15941774 | HCID 15941774 | — |
Reaction Steps
The title compound was prepared (0.137 g, 47%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[7-(2,4-dichlorophenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.125 g, 0.278 mmol) and methylamine (0.086 g, 2.78 mmol). mp 190-192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-8cc210b24f6e4a45a17c0565b4f6c7f9 |
| Source note | uspto-grants-2008_10 |