HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 69108692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86599154 | HCID 86599154 | — |
| Product | HCID 69108692 | HCID 69108692 | — |
Reaction Steps
The title compound was prepared (0.058 g, 79%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[7-(5-chloro-2-methoxyphenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.095 g, 0.213 mmol) and methylamine (0.045 g, 2.1 mmol). mp 201-203° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-6e4b0fb4c014427fa076eb2ac91bfbc0 |
| Source note | uspto-grants-2008_10 |