4-Chloroaniline → HCID 178478206, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 4-chloroaniline (1.35 g) and 2,6-dichloropurine (1 g) in n-butanol (15 ml) was heated at 100° C. for 3 h. The precipitate was filtered off, partitioned between ethyl acetate and aqueous sodium hydroxide solution, the organics dried (MgSO4), and evaporated under reduced pressure. The residue was triturated with ethyl acetate and filtered. Yield 1.04 g

Provenance & Evidence