反应详情

温度

110 °C

A mixture of the product from step (ii) (0.6 g) and sodium thiomethoxide (0.45 g) in dimethylsulphoxide (15 ml) was heated at 110° C. for 4 h. The mixture was partitioned between ethyl acetate and water, the organics washed with water, dried (MgSO4) and evaporated under reduced pressure. Yield 0.45 g

1. customThe mixture was partitioned between ethyl acetate and water
2. washthe organics washed with water
3. dry with materialdried (MgSO4)
4. customevaporated under reduced pressure