HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2116472Generated: October 31, 2026
HCID 68806544, compound → HCID 10065626, compound
https://huagongshe.com/reaction/2116472
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 68806544 | HCID 68806544 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 10065626 | HCID 10065626 | — |
Reaction Steps
4-(3-Phenylsulfonyl-2-chlorophenyl)piperazine-1-carboxylic acid tert-butyl ester (D4A) was dissolved in 8 ml of 1,4-dioxane/4 M HCl 1:1. The mixture was heated at 60° C. for 1 h. The solvent was evaporated in vacuo to give the title product as a colourless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07439245B2 |
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| Source dataset | uspto-grants-2008_10 |
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| ORD ID | ord-5148f87d54244b1fbbd9f864af24b6b1 |
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| Source note | uspto-grants-2008_10 |
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