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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2116532Generated: October 31, 2026

HCID 9948021, compound → HCID 9795116, compound

https://huagongshe.com/reaction/2116532

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 9948021HCID 9948021—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 9795116HCID 979511696%

Reaction Steps

To a stirred solution of the product from Example 1 (101 mg, 0.344 mmol) in MeOH (4 mL) was added a catalytic amount of palladium on carbon. The flask was evacuated of air and placed under a balloon of hydrogen gas. After 1 hr, the mixture was filtered through Celite® and the filtrate was evaporated to provide 85 mg of the title compound (96%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07439242B2
Source datasetuspto-grants-2008_10
ORD IDord-be936f3668a84a2f9b49807acfb5a175
Source noteuspto-grants-2008_10