HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 9948021, compound → HCID 9795116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 9948021 | HCID 9948021 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 9795116 | HCID 9795116 | 96% |
Reaction Steps
To a stirred solution of the product from Example 1 (101 mg, 0.344 mmol) in MeOH (4 mL) was added a catalytic amount of palladium on carbon. The flask was evacuated of air and placed under a balloon of hydrogen gas. After 1 hr, the mixture was filtered through Celite® and the filtrate was evaporated to provide 85 mg of the title compound (96%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-be936f3668a84a2f9b49807acfb5a175 |
| Source note | uspto-grants-2008_10 |