HuagongsheHuagongshe Chemistry Print Report · For research reference only
o-Toluenesulfonyl chloride, 5-nitro- → HCID 9957288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | o-Toluenesulfonyl chloride, 5-nitro- | HCID 8457 | — |
| Reactant | HCID 9948021 | HCID 9948021 | — |
| Product | HCID 9957288 | HCID 9957288 | 89% |
Reaction Steps
The title compound was prepared using the procedure described in Example 3, beginning with 0.1 g of the aniline of Example 1 and 2-methyl-5-nitrobenzenesulfonyl chloride and adding poly(4-vinylpyridine) (250 mg, 60 mesh) to the reaction mixture. After workup, 0.15 g (89%) of the title sulfonamide was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-5f33d16f31214995adcee71c5f4c5170 |
| Source note | uspto-grants-2008_10 |