HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 9848886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 2,6-Dichlorobenzenesulfonylchloride | HCID 522183 | — |
| Reactant | HCID 9948021 | HCID 9948021 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 9848886 | HCID 9848886 | 14% |
Reaction Steps
The title compound was prepared using the procedure described in Example 3, beginning with 0.1 g of the aniline of Example 1 and 2,6-dichlorobenzenesulfonyl chloride and using dimethylformamide as solvent in place of CH2Cl2. After workup, 0.024 g (14%) of the title sulfonamide was obtained
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-65131fee14e04c73aeb92cfcd56adf28 |
| Source note | uspto-grants-2008_10 |