HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dichloro-6-methylbenzenesulfonyl chloride → HCID 9849404, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Reactant | HCID 9948021 | HCID 9948021 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 9849404 | HCID 9849404 | 92% |
Reaction Steps
The title compound was prepared using the alternative procedure described in Example 3. In this manner, 0.1 g of the aniline of Example 1 was combined with 2,4-dichloro-6-methylbenzenesulfonyl chloride and polyvinyl pyridine to provide 0.162 g (92%) of the title sulfonamide after chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-77db6b2007664705bf3d2f5f2d90a4be |
| Source note | uspto-grants-2008_10 |