HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenesulfonyl chloride, 2,4-dichloro- → HCID 22993864, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenesulfonyl chloride, 2,4-dichloro- | HCID 204419 | — |
| Reactant | HCID 22993850 | HCID 22993850 | — |
| Product | HCID 22993864 | HCID 22993864 | — |
Reaction Steps
Using the method of Example 17.4, 4-(3-chloro-5-pyridyloxy)-3-aminobenzotrifluoride (0.4 g) and 2,4-dichlorobenzenesulfonyl chloride ((0.38 g) were combined to provide the title compound (0.26 g), as a crystalline solid following flash chromatography and trituration with ether. mp 150-151.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-71d7e6918f5743979ebdf79b7669f6b6 |
| Source note | uspto-grants-2008_10 |