Acetaldehyde → HCID 69305311, compound

HRID 2116805Notes

Reaction equation

[CH:1](=[O:3])[CH3:2].[CH3:4][CH2:5][CH2:6][CH2:7][CH2:8][CH3:9].C(OCC)(=[O:12])C>>[OH:3][CH:1]([C:6]1[C:7](=[O:12])[CH2:8][CH2:9][C:5]=1[CH3:4])[CH3:2]

Participants

Reactant 3

HCID 177Acetaldehyde

HCID 8058Hexane

HCID 8857Ethyl Acetate

Product 1

HCID 69305311HCID 69305311, compoundYield 95%

Procedure

The same procedure as in Example 14 was carried out using acetaldehyde instead of formaldehyde. The target compound was obtained by column chromatography (hexane:ethyl acetate=1:1) (yield: 95%).

Sources & evidence

ORD record: ord-aad656d1ade34eabb39dfacab73e7b2e
Source dataset: uspto-grants-2008_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07439378B2

Reaction notes

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