HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxyamine hydrochloride → HCID 86609838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 69290738 | HCID 69290738 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86609838 | HCID 86609838 | — |
Reaction Steps
In a manner similar to that of Example 1.g, by reaction of 370 mg (0.8 mmol) of allyl 4-{2-[4-(acetylethylamino)-3-tert-butylphenyl]-2-oxoethoxy}-2-hydroxybenzoate with 284 mg (4 mmol) of hydroxylamine hydrochloride and 320 μl of pyridine. A yellowish paste is obtained (m=380 mg, yield=99%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439396B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-418f55cce90c416787f3d455064b7436 |
| Source note | uspto-grants-2008_10 |