Diethylamine → HCID 178464165, compound

Participants

Reaction Steps

3.42 g (46.8 mmol) of diethylamine are added with stirring and ice-cooling to 5.00 g (21.3 mmol) of bis(dimethylamino)chlorocarbenium perchlorate. The reaction mixture is subsequently stirred for 1 hour at room temperature and subsequently added to 20 ml of water. The organic phase is separated off and washed with 20 ml of water. The liquid is subsequently dried at 50° C. under reduced pressure (7.0 Pa), giving 5.17 g of N,N,N′,N′-tetramethyl-N″,N″-diethylguanidinium perchlorate, corresponding to a yield of 89.6%.

Provenance & Evidence